(R)-2-乙酰氧基-2-苯乙酸合成路线 (共 15 条)
参考文献
Corey, E. J.; Naef, Reto; Hannon, Francis J.
Journal of the American Chemical Society, 1986 , vol. 108, # 22 p. 7114 - 7116
反应条件
1: With sodium carbonate in aq. phosphate buffer T=30°C; pH=6.5; 15 h; Enzymatic reaction; 2: With sulfuric acid enantioselective reaction;
参考文献
Ma, Bao-Di; Kong, Xu-Dong; Yu, Hui-Lei; Zhang, Zhi-Jun; Dou, Shuai; Xu, Yan-Peng; Ni, Yan; Xu, Jian-He
ACS Catalysis, 2014 , vol. 4, # 3 p. 1026 - 1031
反应条件
air in ethanol; acetonitrile Irradiation;
参考文献
Ashraf, M. Arfan; Russell, Alexander G.; Wharton, Christopher W.; Snaith, John S.
Tetrahedron, 2007 , vol. 63, # 3 p. 586 - 593
反应条件
N-isopropylcarbamoyl-derivatized cyclofructan-6 column in ethanol; n-heptane; trifluoroacetic acid T=20°C; Resolution of racemate;
参考文献
BOARD OF REGENTS, THE UNIVERSITY OF TEXAS SYSTEM; ARMSTRONG, Daniel, W.; PING, Sun; BREITBACH, Zachary, S.; WANG, Chunlei
Patent: WO2010/148191 A2, 2010 ;
Location in patent: Page/Page column 45-49; 51 ;
反应条件
sodium periodate; ruthenium trichloride in tetrachloromethane; water; acetonitrile 1 h; Ambient temperature;
参考文献
Kitano, Yasunori; Kusakabe, Masato; Kobayashi, Yuichi; Sato, Fumie
Journal of Organic Chemistry, 1989 , vol. 54, # 4 p. 994 - 996
反应条件
2: 90 percent / pyridine 3: NaIO4 / RuCl3*3H2O / H2O; CCl4; acetonitrile / 1 h / Ambient temperature View Scheme
参考文献
Kitano, Yasunori; Kusakabe, Masato; Kobayashi, Yuichi; Sato, Fumie
Journal of Organic Chemistry, 1989 , vol. 54, # 4 p. 994 - 996
反应条件
lithium hydroxide; dihydrogen peroxide in tetrahydrofuran; water
参考文献
Chavda, Sameer; Coulbeck, Elliot; Eames, Jason
Tetrahedron Letters, 2008 , vol. 49, # 52 p. 7398 - 7402
反应条件
ruthenium trichloride; sodium periodate in tetrachloromethane; water; acetonitrile 1 h; Ambient temperature; Yield given;
参考文献
Kusakabe, Masato; Kitano, Yasunori; Kobayashi, Yuichi; Sato, Fumie
Journal of Organic Chemistry, 1989 , vol. 54, # 9 p. 2085 - 2091
反应条件
1: 38 percent 2: pyridine / 12 h / Ambient temperature 3: NaIO4, RuCl3*3H2O / CCl4; acetonitrile; H2O / 1 h / Ambient temperature View Scheme
参考文献
Kusakabe, Masato; Kitano, Yasunori; Kobayashi, Yuichi; Sato, Fumie
Journal of Organic Chemistry, 1989 , vol. 54, # 9 p. 2085 - 2091
反应条件
1: pyridine / 12 h / Ambient temperature 2: NaIO4, RuCl3*3H2O / CCl4; acetonitrile; H2O / 1 h / Ambient temperature View Scheme
参考文献
Kusakabe, Masato; Kitano, Yasunori; Kobayashi, Yuichi; Sato, Fumie
Journal of Organic Chemistry, 1989 , vol. 54, # 9 p. 2085 - 2091