Baldwin, Jack E.; Field, Robert A.; Lawrence, Christopher C.; Merritt, Kirsten D.; Schofield, Christopher J.
Tetrahedron Letters, 1993 , vol. 34, # 46 p. 7489 - 7492
1: 90 percent / sodium borohydride / methanol / 3.5 h / 0 °C 2: 62 percent / aq. NaOH / diethyl ether / 24 h 3: 36 percent / lithium triethylborodeuteride / tetrahydrofuran / 24 h / Heating 4: trifluoroacetic acid / 0.5 h 5: TES buffer, iron(II)ammonium sulphate, 2-oxoglutarate, proline 4-hydroxylase / 4 h / 26 °C / incubation View Scheme
参考文献
Baldwin, Jack E.; Field, Robert A.; Lawrence, Christopher C.; Merritt, Kirsten D.; Schofield, Christopher J.
Tetrahedron Letters, 1993 , vol. 34, # 46 p. 7489 - 7492
1: 62 percent / aq. NaOH / diethyl ether / 24 h 2: 36 percent / lithium triethylborodeuteride / tetrahydrofuran / 24 h / Heating 3: trifluoroacetic acid / 0.5 h 4: TES buffer, iron(II)ammonium sulphate, 2-oxoglutarate, proline 4-hydroxylase / 4 h / 26 °C / incubation View Scheme
参考文献
Baldwin, Jack E.; Field, Robert A.; Lawrence, Christopher C.; Merritt, Kirsten D.; Schofield, Christopher J.
Tetrahedron Letters, 1993 , vol. 34, # 46 p. 7489 - 7492
1: 36 percent / lithium triethylborodeuteride / tetrahydrofuran / 24 h / Heating 2: trifluoroacetic acid / 0.5 h 3: TES buffer, iron(II)ammonium sulphate, 2-oxoglutarate, proline 4-hydroxylase / 4 h / 26 °C / incubation View Scheme
参考文献
Baldwin, Jack E.; Field, Robert A.; Lawrence, Christopher C.; Merritt, Kirsten D.; Schofield, Christopher J.
Tetrahedron Letters, 1993 , vol. 34, # 46 p. 7489 - 7492
