(S)-1-(3-吡啶基)乙醇合成路线 (共 22 条)
反应条件
(S)-(4-tert-butyl-2-thioxothiazolidin-3-yl)[4-(dimethylamino)pyridin-3-yl]methanone; triethylamine T=-30°C; 48 h;
参考文献
Tetrahedron Letters, , vol. 46, # 13 p. 2239 - 2242
反应条件
1: 36 percent / H2O / 95 h / 27 °C / baker's yeast 2: 47 percent / Raney Ni View Scheme
参考文献
Heterocycles, , vol. 30, # 2 p. 871 - 874
反应条件
in various solvent(s) 40 h; Ambient temperaturelipase from Pseudomonas sp. (SAM II);
参考文献
Tetrahedron: Asymmetry, , vol. 3, # 7 p. 827 - 830
反应条件
(S)-(-)-2-lt;2',2'-dimethyl-1'-(2''-pyridyl)propoxygt;-1,1-di-(α-naphthyl)ethanol in hexane; toluene 1 h; Ambient temperature; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Chemistry Letters, , # 7 p. 1337 - 1340
反应条件
1: isopropyl alcohol With [RuCl2(η6-p-cymene)(R)-N-((1-phenylethyl)carbamothioyl)benzamide]; potassium hydroxide T=20 - 82°C; 0.166667 h; Inert atmosphere; 2: 3-acetyl-pyridine T=85°C; 24 h; Inert atmosphere; Reagent/catalyst;
参考文献
Organometallics, , vol. 33, # 2 p. 540 - 550
反应条件
air; cells of Geotrichum candidum IFO5767 in water T=30°C; 24 h; Product distribution;
参考文献
Tetrahedron Asymmetry, , vol. 12, # 22 p. 3147 - 3153
反应条件
Pseudomonas putida UV4; oxygen Enzymatic reaction; Title compound not separated from byproducts;
参考文献
Tetrahedron Asymmetry, , vol. 13, # 20 p. 2201 - 2204
参考文献
Tetrahedron: Asymmetry, , vol. 3, # 7 p. 827 - 830
Tetrahedron: Asymmetry, , vol. 5, # 7 p. 1363 - 1366
Tetrahedron Asymmetry, , vol. 8, # 6 p. 935 - 948
Bioorganic Chemistry, , vol. 27, # 1 p. 3 - 19
反应条件
(1R,2R)-α,α,α',α'-tetraphenyl-1,2-cyclohexanedimethanol; TiF4 in CH3CN 1) THF, hexane, 0 deg C to RT, 20 min, 2) THF, hexane, 20 min, 3) THF, hexane, -10 deg C, 12 h then warm to RT; Yield givenMultistep reaction. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Tetrahedron Letters, , vol. 39, # 52 p. 9593 - 9596
反应条件
in toluene T=25°C; 16 h; Yield given. Yields of byproduct given;
参考文献
Gaertner, Holger; Salz, Ulrich; Ruechardt, Christoph
Angewandte Chemie, 1984 , vol. 96, # 2 p. 166 - 167