(S)-1-(3-吡啶基)乙醇合成路线 (共 22 条)
反应条件
dodecacarbonyltriiron; C52H58N4P2; hydrogen; potassium hydroxide in methanol T=45°C; P=37503.8 Torr; 5 h; enantioselective reaction;
参考文献
Journal of the American Chemical Society, , vol. 136, # 10 p. 4031 - 4039
反应条件
in water T=33°C; 26 h; baker's yeast; Title compound not separated from byproducts;
参考文献
Heterocycles, , vol. 26, # 12 p. 3051 - 3054
反应条件
Rhizopus nigricans (sterile potato dextrose medium) in tetrahydrofuran 16 h; Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Journal of Organic Chemistry, , vol. 48, # 18 p. 3017 - 3021
反应条件
Lipase PS-C in di-isopropyl ether T=35°C; 6.5 h;
参考文献
Chemistry - A European Journal, , vol. 12, # 36 p. 9228 - 9237
反应条件
nicotinamide; sodium phosphate buffer; G6P; NADP; magnesium chloride in water T=37°C; 1 h; biotransformation with phenobarbital-pretreated rat-liver (S-9);
参考文献
Heterocycles, , vol. 42, # 2 p. 831 - 836
反应条件
tris(hydroxymethyl)methylamine hydrochloride in water T=30°C; pH=8.5; 40 h; optical yield given as percent eeenantioselective reaction;
参考文献
Journal of Molecular Catalysis B: Enzymatic, , vol. 64, # 1-2 p. 48 - 52
反应条件
1: 37 percent / aq. NaOH / 120 h / lipase from Pseudomonas sp. (SAM II), phosphate buffer pH 7.0 2: K2CO3 / methanol / 0.5 h / Ambient temperature View Scheme
参考文献
Tetrahedron: Asymmetry, , vol. 3, # 7 p. 827 - 830
反应条件
potassium carbonate in methanol 0.5 h; Ambient temperature;
参考文献
Tetrahedron: Asymmetry, , vol. 3, # 7 p. 827 - 830
参考文献
Heterocycles, , vol. 30, # 2 p. 871 - 874
反应条件
sodium hydroxide; Candida rugosa lipase E.(1)C3113 type VII in phosphate buffer T=20°C; pH=7.2; 22 h; Title compound not separated from byproducts.;
参考文献
Journal of the Chemical Society, Perkin Transactions 1, , # 24 p. 4439 - 4444