[(亚苄基胺)甲基]磷酸二乙酯合成路线 (共 7 条)
反应条件
sodium sulfate; triethylamine in dichloromethane Ambient temperature;
参考文献
Wu, Shi-Hui; Sun, Wei-Quan; Zhang, Dan-Wei; Shu, Lian-He; Wu, Hou-Ming; Xu, Jing-Fei; Lao, Xia-Fei
Journal of the Chemical Society - Perkin Transactions 1, 1998 , # 10 p. 1733 - 1738
反应条件
trimethylsilyl trifluoromethanesulfonate in dichloromethane Ambient temperature;
参考文献
Morimoto, Toshiaki; Sekiya, Minoru
Chemistry Letters, 1985 , p. 1371 - 1372
反应条件
1: H2 / Pd-C / ethanol View Scheme
参考文献
Ratcliffe; Christensen
Tetrahedron Letters, 1973 , vol. No. 46, p. 4645 - 4648
反应条件
1: diethyl α-azidomethylphosphonate With triphenylphosphine in benzene T=20°C; 3 h; 2: benzaldehyde in benzene T=20°C; 20 h;
参考文献
Gajda; Janik
Polish Journal of Chemistry, 2005 , vol. 79, # 3 p. 493 - 498
反应条件
1: NaH / tetrahydrofuran / 2 h / 45 °C 2: NaBH4 / ethanol / 1 h / 50 °C 3: aq. HCl / 1.5 h / 80 - 85 °C View Scheme
参考文献
Heymes, A.; Chekroun, I.
Synthesis, 1987 , # 3 p. 245 - 249
反应条件
1: NaH / tetrahydrofuran / 2 h / 45 °C
2: NaBH4 / ethanol / 1 h / 50 °C
View Scheme
参考文献
Heymes, A.; Chekroun, I.
Synthesis, 1987 , # 3 p. 245 - 249
反应条件
(i) NaH, THF, (ii) /BRN= 605842/; Multistep reaction;
参考文献
Dehnel,A. et al.
Synthesis, 1977 , p. 474 - 476