5-(2-氯苯基)1H-四唑合成路线 （共 11 条）
反应条件
diethylaluminium azide in xylene T=50°C; 27 h;
参考文献
Aureggi, Valentina; Sedelmeier, Gottfried
Angewandte Chemie - International Edition, 2007 , vol. 46, # 44 p. 8440 - 8444
反应条件
sodium azide; tetrachlorosilane in acetonitrile T=20 - 82°C; 1.66667 h;
参考文献
El-Ahl, Abdel-Aziz S.; Amer, Fatty A.; Elbeheery, Akram H.
Phosphorus, Sulfur and Silicon and the Related Elements, 2011 , vol. 186, # 11 p. 2226 - 2235
反应条件
triazidochlorosilane in acetonitrile 1.5 h; Heating;
参考文献
El-Ahl, Abdel-Aziz S.; Elmorsy, Saad S.; Elbeheery, Akram H.; Amer, Fathy A.
Tetrahedron Letters, 1997 , vol. 38, # 7 p. 1257 - 1260
反应条件
hydrogenchloride; sodium nitrite 1.) pyridine, from ice-cooled solution to room t. over 12 h; 2.) -5 - 0 degC, 1 h; Yield given. Multistep reaction;
参考文献
Boivin, Jean; Husinec, Suren; Zard, Samir Z.
Tetrahedron, 1995 , vol. 51, # 43 p. 11737 - 11742
参考文献
Stolle
Journal fuer Praktische Chemie (Leipzig), 1933 , vol. <2> 138, p. 1,14
反应条件
1: tetrachloromethane / 50 °C / Einleiten von Chlor 2: ethanol; NaN3 3: aq.-ethanolic HCl 4: aqueous NaNO2 View Scheme
参考文献
Stolle
Journal fuer Praktische Chemie (Leipzig), 1933 , vol. <2> 138, p. 1,14
反应条件
1: ethanol; NaN3 2: aq.-ethanolic HCl 3: aqueous NaNO2 View Scheme
参考文献
Stolle
Journal fuer Praktische Chemie (Leipzig), 1933 , vol. <2> 138, p. 1,14
反应条件
in dimethylsulfoxide-d6; chloroform-d1 Equilibrium constant;
参考文献
Butler, Richard N.; Garvin, Victor C.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1981 , p. 390 - 393
反应条件
in dimethylsulfoxide-d6; chloroform-d1 Equilibrium constant;
参考文献
Butler, Richard N.; Garvin, Victor C.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1981 , p. 390 - 393
反应条件
in o-xylene T=120 - 125°C; 4 h;
参考文献
Baranov; Tsypin; Malin; Laskin
Russian Journal of Applied Chemistry, 2005 , vol. 78, # 5 p. 773 - 775
