1: 82 percent / NEt3 / toluene / 48 h / Heating 2: 82 percent / LiAlH4 / diethyl ether / 10 h / Heating 3: 69 percent / 3 h / 70 °C 4: neat (no solvent) / 134.9 °C / lgA, EA, ΔH(excit.), ΔS(excit.), ΔG(excit.), ΔrH View Scheme

1: 82 percent / LiAlH4 / diethyl ether / 10 h / Heating 2: 69 percent / 3 h / 70 °C 3: neat (no solvent) / 134.9 °C / lgA, EA, ΔH(excit.), ΔS(excit.), ΔG(excit.), ΔrH View Scheme

1: 69 percent / 3 h / 70 °C 2: neat (no solvent) / 134.9 °C / lgA, EA, ΔH(excit.), ΔS(excit.), ΔG(excit.), ΔrH View Scheme

T=135°C; 67 h;

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