3-苯基二硫代肼基甲酸甲酯合成路线 (共 12 条)
反应条件
in ethanol; water
boiling soln. of Pt-complex in water was added to soln. of ligand (molar ratio 1:2) in EtOH, boiled for 10 min; react. can be carried out underN2 in basic media; filtered off, washed with hot water-EtOH, dried in vac. over P2O5; elem. anal.;
参考文献
Battistoni, Claudio; Giuliani, Anna Maria; Paparazzo, Ernesto; Tarli, Franco
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), 1984 , p. 1293 - 1300
反应条件
1: 72 h / Heating
2: 53.23 g / oxygen; diethylamine / 24 h / 20 °C
View Scheme
参考文献
Nielsen, Kim T.; Bechgaard, Klaus; Krebs, Frederik C.
Macromolecules, 2005 , vol. 38, # 3 p. 658 - 659