2-(9-十二碳炔基氧基)四氢-2H-吡喃合成路线 （共 3 条）
反应条件
1: 2.9 g / TsOH / methanol; H2O / 20 h 2: LiAlH4 / tetrahydrofuran; bis-(2-methoxy-ethyl) ether / 36 h / 140 °C View Scheme
参考文献
Kamezawa, Makoto; Tachibana, Hojun; Ohtani, Takehiko; Naoshima, Yoshinobu
Bioscience, Biotechnology, and Biochemistry, 1993 , vol. 57, # 11 p. 1962 - 1963
反应条件
1: 2.9 g / TsOH / methanol; H2O / 20 h 2: LiAlH4 / tetrahydrofuran; bis-(2-methoxy-ethyl) ether / 36 h / 140 °C 3: 1.1 g / pyridine / 24 h / Ambient temperature View Scheme
参考文献
Odinokov; Botsman; Gladysheva
Chemistry of Natural Compounds, 1996 , vol. 32, # 3 p. 381 - 383
反应条件
toluene-4-sulfonic acid in methanol
T=60 - 65°C; 4 h;
参考文献
Kamezawa, Makoto; Tachibana, Hojun; Ohtani, Takehiko; Naoshima, Yoshinobu
Bioscience, Biotechnology, and Biochemistry, 1993 , vol. 57, # 11 p. 1962 - 1963
