oxygen; GNO3; hydrazine hydrate in ethanol T=80°C; P=760.051 Torr; 16 h;

1: H2SO4 / Heating 2: LiAlH4 / diethyl ether 3: polyphosphoric acid / 1 h / 220 °C View Scheme

1: PCl5 / anschliessendes Behandeln mit NH3 in Benzol 2: Behandeln des Reaktionsprodukts mit wss. NaOH View Scheme

sulfuric acid T=0 - 5°C; 0.0833333 h;

1: LiAlH4 2: 85 percent / Jones' reagent 3: 63 percent / NaOEt / ethanol / -10 °C 4: 56 percent / 3-chloroperbenzoic acid (80percent) / CH2Cl2 / Ambient temperature 5: 40 percent / triethyl phosphite / tetrahydrofuran / 12 h / Ambient temperature 6: toluene / 2 h / Heating View Scheme

bis-[(trifluoroacetoxy)iodo]benzene in acetonitrile T=20°C; Inert atmosphere;

diphenyl diselenide; bis-[(trifluoroacetoxy)iodo]benzene in acetonitrile T=20°C; 1 h; Inert atmosphere; Mechanism; TimeConcentration;

1: LiAlH4 2: 85 percent / Jones' reagent View Scheme