(S)-1-对甲苯磺酰氧基-2,3-丙二醇合成路线 （共 21 条）
反应条件
indium trifluoromethanesulfonate in water; acetonitrile T=100°C; 0.0833333 h; Microwave irradiation; chemoselective reaction;
参考文献
Golden, Kathryn C.; Gregg, Brian T.; Quinn, John F.
Tetrahedron Letters, 2010 , vol. 51, # 31 p. 4010 - 4013
反应条件
hydrogenchloride in methanol 6 h;
参考文献
Leftheris, Katerina; Goodman, Murray
Journal of Medicinal Chemistry, 1990 , vol. 33, # 1 p. 216 - 223
反应条件
hydrogen; palladium on activated charcoal in ethanol
参考文献
Kurimura; Takemoto; Achiwa
Chemical and Pharmaceutical Bulletin, 1991 , vol. 39, # 10 p. 2590 - 2596
反应条件
toluene-4-sulfonic acid in methanol T=60°C; 3 h;
参考文献
Bosetti, Aldo; Bianchi, Daniele; Cesti, Pietro; Golini, Paolo; Spezia, Sandro
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1992 , # 18 p. 2395 - 2398
反应条件
hydrogen; palladium on activated charcoal in methanol
参考文献
Nelson,W.L. et al.
Journal of Organic Chemistry, 1977 , vol. 42, p. 1006 - 1012
反应条件
potassium dioxotetrahydroxoosmate(VI); potassium carbonate; potassium hexacyanoferrate(III); 1,4-bis(dihydroquinidinyl)anthraquinone in water; tert-butyl alcohol T=0°C; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Becker, Heinrich; Sharpless, K. Barry
Angewandte Chemie, 1996 , vol. 108, # 4 p. 447 - 449
反应条件
triethylamine in chloroform 12 h;
参考文献
Shiratsuchi; Kawamura; Akashi; Ishihama; Nakamura; Takenaka
Chemical and Pharmaceutical Bulletin, 1987 , vol. 35, # 9 p. 3691 - 3698
反应条件
toluene-4-sulfonic acid; palladium on activated charcoal in methanol; water 18 h; Heating; Yield given;
参考文献
Wirz, Beat; Schmid, Rudolf; Foricher, Joseph
Tetrahedron: Asymmetry, 1992 , vol. 3, # 1 p. 137 - 142
反应条件
1: 2 M aq. KOH / methanol / 1 h / 0 °C 2: p-toluenesulfonic acid / 10 percent Pd/C / methanol; H2O / 18 h / Heating View Scheme
参考文献
Wirz, Beat; Schmid, Rudolf; Foricher, Joseph
Tetrahedron: Asymmetry, 1992 , vol. 3, # 1 p. 137 - 142
反应条件
1: 98 percent / 6N HCl / methanol / 8 h / 60 °C 2: 99 percent / H2 / 5percent Pd/C / ethanol View Scheme
参考文献
Kurimura; Takemoto; Achiwa
Chemical and Pharmaceutical Bulletin, 1991 , vol. 39, # 10 p. 2590 - 2596
