内消旋-1,2-双(对甲苯基)乙二胺合成路线 (共 5 条)
反应条件
1: With ammonium acetate T=120°C; 3 h; 2: With sulfuric acid; water T=170°C; 12 h;
参考文献
Mendez-Sanchez, Daniel; Rios-Lombardia, Nicolas; Garcia-Granda, Santiago; Montejo-Bernardo, Jose; Fernandez-Gonzalez, Alfonso; Gotor, Vicente; Gotor-Fernandez, Vicente
Tetrahedron Asymmetry, 2014 , vol. 25, # 4 p. 381 - 386
反应条件
methanesulfonic acid; zinc in tetrahydrofuran T=25°C; reduction; 8 h;
参考文献
Kise, Naoki; Ueda, Nasuo
Tetrahedron Letters, 2001 , vol. 42, # 12 p. 2365 - 2368
反应条件
methanesulfonic acid; zinc in acetonitrile T=25°C; reduction;
参考文献
Kise, Naoki; Ueda, Nasuo
Tetrahedron Letters, 2001 , vol. 42, # 12 p. 2365 - 2368
反应条件
titanium tetrachloride; zinc in tetrahydrofuran T=25°C; reduction;
参考文献
Kise, Naoki; Ueda, Nasuo
Tetrahedron Letters, 2001 , vol. 42, # 12 p. 2365 - 2368
参考文献
Voegtle,F.; Goldschmitt,E.
Chemische Berichte, 1976 , vol. 109, p. 1 - 40