in tetrahydrofuran; methanol 96 h; Inert atmosphereMolecular sieveReflux;
参考文献
Li, Jie; Lutz, Martin; Spek, Anthony L.; Van Klink, Gerard P.M.; Van Koten, Gerard; Klein Gebbink, Robertus J.M.
Journal of Organometallic Chemistry, 2010 , vol. 695, # 24 p. 2618 - 2628
1.1: triethylamine / dichloromethane / 24 h / 20 °C 2.1: n-butyllithium / tetrahydrofuran / 1 h / -78 °C 2.2: 5 h / 20 °C 3.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 2 h / 20 °C View Scheme
参考文献
Sieber, Frank; Wentworth Jr., Paul; Janda, Kim D.
Molecules, 2000 , vol. 5, # 8 p. 1018 - 1032
