4-溴-2,3-二甲基苯甲醚合成路线 （共 9 条）
反应条件
N-bromosuccinmide in tetrachloromethane 1 h; Ambient temperature;
参考文献
Box, Vernon, G. S.; Yiannikouros, George P.
Heterocycles, 1990 , vol. 31, # 7 p. 1261 - 1270
反应条件
potassium carbonate in acetone T=70°C; 6 h;
参考文献
Takeuchi, Makoto; Kurahashi, Takuya; Matsubara, Seijiro
Chemistry Letters, 2012 , vol. 41, # 12 p. 1566 - 1568
反应条件
N-bromosuccinmide in tetrachloromethane 36 h; Heating; Yields of byproduct given;
参考文献
Goldberg, Yuri; Bensimon, Corrine; Alper, Howard
Journal of Organic Chemistry, 1992 , vol. 57, # 23 p. 6374 - 6376
反应条件
1: 84 percent / aq. NaOH 2: 91 percent / Br2 / acetic acid View Scheme
参考文献
Short; Stromberg; Wiles
Journal of the Chemical Society, 1936 , p. 319,321
反应条件
N-bromosuccinmide in tetrachloromethane 0.5 h; HeatingIrradiation; Title compound not separated from byproducts;
参考文献
Gruter, Gert-Jan M.; Akkerman, Otto S.; Bickelhaupt, Friedrich
Journal of Organic Chemistry, 1994 , vol. 59, # 16 p. 4473 - 4481
参考文献
Baliah,V.; Uma,M.
Recueil des Travaux Chimiques des Pays-Bas, 1961 , vol. 80, p. 139 - 148
反应条件
1: 90 percent / NaOMe; CuI / dimethylformamide / 24 h / Heating 2: 77 percent / NBS; benzoyl peroxide / CCl4 / 1.5 h / Irradiation; reflux View Scheme
参考文献
Eskildsen, Jorgen; Christensen, Trine; Reenberg, Theis; Larsen, Uffe; Christensen, Jorn B.
Organic Preparations and Procedures International, 2000 , vol. 32, # 4 p. 398 - 400
反应条件
1: 100 percent / N-bromosuccinimide (NBS) / CCl4 / Heating; Irradiation 2: 95 percent / sodium acetate, glacial acetic acid / 3 h / Heating 3: 96 percent / potassium carbonate / methanol; H2O / 4 h / Ambient temperature 4: 90 percent / Jones reagent / acetone / Heating View Scheme
参考文献
Box, Vernon, G. S.; Yiannikouros, George P.
Heterocycles, 1990 , vol. 31, # 7 p. 1261 - 1270
反应条件
copper(l) iodide; sodium methylate in N,N-dimethyl-formamide
Substitution; 24 h; Heating;
参考文献
Eskildsen, Jorgen; Christensen, Trine; Reenberg, Theis; Larsen, Uffe; Christensen, Jorn B.
Organic Preparations and Procedures International, 2000 , vol. 32, # 4 p. 398 - 400
