2,3,4-三甲氧基苯胺合成路线 （共 10 条）
反应条件
palladium 10 on activated carbon; hydrogen in ethyl acetate
P=1551.49 Torr; 6 h;
参考文献
Maiti, Arup; Reddy, P. V. Narasimha; Sturdy, Megan; Marler, Laura; Pegan, Scott D.; Mesecar, Andrew D.; Pezzuto, John M.; Cushman, Mark
Journal of Medicinal Chemistry, 2009 , vol. 52, # 7 p. 1873 - 1884
参考文献
Lions
Journal and Proceedings of the Royal Society of New South Wales, 1929 , vol. 63, p. 168,170
反应条件
hydrogenchloride; tin
参考文献
Baker; Smith
Journal of the Chemical Society, 1931 , p. 2542,2546
反应条件
1: glacial acetic acid; acetic acid anhydride; acetic acid; aqueous nitric acid / <5
2: K2CO3; xylene / 130 °C
3: tin; aqueous hydrochloric acid
View Scheme
参考文献
Baker; Smith
Journal of the Chemical Society, 1931 , p. 2542,2546
参考文献
Graebe; Suter
Justus Liebigs Annalen der Chemie, 1905 , vol. 340, p. 230
反应条件
1: diluted alkaline solution
2: NaOH-solution / die Loesung unter Zusatz von Aetznatron bezw. konz. Natronlauge kochen
3: benzene; PCl5 / man leitet in erhaltene Loesung Ammoniak
4: hypochlorite
View Scheme
参考文献
Graebe; Suter
Justus Liebigs Annalen der Chemie, 1905 , vol. 340, p. 230
反应条件
1: NaOH-solution / die Loesung unter Zusatz von Aetznatron bezw. konz. Natronlauge kochen
2: benzene; PCl5 / man leitet in erhaltene Loesung Ammoniak
3: hypochlorite
View Scheme
参考文献
Graebe; Suter
Justus Liebigs Annalen der Chemie, 1905 , vol. 340, p. 230
反应条件
1: benzene; PCl5 / man leitet in erhaltene Loesung Ammoniak
2: hypochlorite
View Scheme
参考文献
Graebe; Suter
Justus Liebigs Annalen der Chemie, 1905 , vol. 340, p. 230
反应条件
1: K2CO3; xylene / 130 °C
2: tin; aqueous hydrochloric acid
View Scheme
参考文献
Baker; Smith
Journal of the Chemical Society, 1931 , p. 2542,2546
反应条件
1: concentrated sulfuric acid; arsenic (V)-oxide
2: sodium; ethanol
View Scheme
参考文献
Taylor
Journal of the Chemical Society, 1951 , p. 1150,1155
