educts separately condensed into a reactor held at -196°C, then allowed to react for 35 min at room temp.; volatile products were removed and analyzed, identification by NMR;
参考文献
Krause, L. J.; Morrison, J. A.
Inorganic Chemistry, 1980 , vol. 19, p. 604 - 607
educts separately condensed into a reactor held at -196°C, then allowed to react for 15 min at room temp., in the presence of substoich.amt. of (CH3)2Cd; volatile products were removed and analyzed, identification by NMR;
educts separately condensed into a reactor held at -196°C, then allowed to react for 15 min at room temp., at 10-fold excess of (CH3)2Cd; volatile products were removed and analyzed, identification by NMR;
参考文献
Krause, L. J.; Morrison, J. A.
Inorganic Chemistry, 1980 , vol. 19, p. 604 - 607