反应条件
1: 1.) butyllithium / 1.) THF, hexane, -70 deg C, 15 min, 2.) a) -70 deg C, 5 h, b) from -70 deg to RT, 1.5 h, c) RT, 15 h 2: 90 percent / H2 / 2percent Pd-C / hexane / 120 h / Ambient temperature 3: 99.9 percent / KOH / methanol; H2O / 1.) 50 deg C, 6 h, 2.) RT, 15 h View Scheme
参考文献
Odinokov, V. N.; Akhmetova, V. R.; Khasanov, Kh. D.; Abduvakhabov, A. A.; Tolstikov, G. A.
Journal of Organic Chemistry USSR (English Translation), 1990 , vol. 26, # 7.1 p. 1209 - 1210
Zhurnal Organicheskoi Khimii, 1990 , vol. 26, # 7 p. 1402 - 1404
