3-氯-6-硝基-1H-吲唑合成路线 （共 7 条）
反应条件
1: With sodium hydroxide in water T=0°C; 0.25 h; Heating; 2: With sodium hypochlorite in water T=0°C; 5 h; 3: With hydrogenchloride in water pH=7;
参考文献
Souers, Andrew J.; Collins, Christine A.; Gao, Ju; Judd, Andrew S.; Kym, Philip R.; Mulhern, Mathew M.; Sham, Hing L.; Wodka, Dariusz
Patent: US2005/277638 A1, 2005 ;
Location in patent: Page/Page column 49 ;
US 20050277638 A1
反应条件
1: With sodium hydroxide in water Heating / reflux; 2: With sodium hypochlorite in water T=0°C; pH=7; 5.25 h; 3: With hydrogenchloride in water
参考文献
Souers, Andrew J.; Collins, Christine A.; Gao, Ju; Judd, Andrew S.; Kym, Philip R.; Mulhern, Mathew M.; Sham, Hing L.; Vasudevan, Anil; Wodka, Dariusz
Patent: US2005/137243 A1, 2005 ;
Location in patent: Page/Page column 48 ;
US 20050137243 A1
反应条件
hydrogenchloride in tetrahydrofuran; water
参考文献
Stein, Philip D.; O'Connor, Stephen P.; Shi, Yan; Li, Chi
Patent: US2002/25957 A1, 2002 ;
反应条件
diethylamine in ethanol 4 h; Irradiation;
参考文献
Bouchet, P.; Lazaro, R.; Benchidmi, M.; Elguero, J.
Tetrahedron, 1980 , vol. 36, p. 3523 - 3534
反应条件
phosphorus trichoride
参考文献
Davies
Journal of the Chemical Society, 1955 , p. 2412,2419
反应条件
palladium monocarbide in methanol
参考文献
Stein, Philip D.; O'Connor, Stephen P.; Shi, Yan; Li, Chi
Patent: US2002/25957 A1, 2002 ;
反应条件
pyridine
1 h; Heating;
参考文献
Ang, Kiah H.; Donati, Cosimo; Donkor, Augustine; Prager, Rolf H.
Australian Journal of Chemistry, 1992 , vol. 45, # 12 p. 2037 - 2048
