(±)-反-1,2-环戊二醇合成路线 （共 48 条）
反应条件
ytterbium trichloride in tetrahydrofuran Acetylation;
参考文献
Tetrahedron Letters, , vol. 41, # 15 p. 2687 - 2690
反应条件
sodium periodate in water; ethyl acetate; acetonitrile T=0°C; 2 h;
参考文献
Synlett, , # 5 p. 739 - 742
参考文献
Justus Liebigs Annalen der Chemie, , vol. 518, p. 1,25
参考文献
DE717203 , ;
DRP/DRBP Org.Chem.
参考文献
Helvetica Chimica Acta, , vol. 36, p. 268,273
反应条件
1: 91 percent / triethylamine / CH2Cl2 / 7 h / 0 - 20 °C 2: 86 percent / sodium azide / dimethylformamide / 24 h / 85 °C 3: 90 percent / hydrogen / 10 percent Pd/C / ethanol / 6 h / 20 °C View Scheme
参考文献
Gouin, Sebastien G; Gestin, Jean-Francois; Joly, Kevin; Loussouarn, Anthony; Reliquet, Alain; Claude Meslin, Jean; Deniaud, David
Tetrahedron, 2002 , vol. 58, # 6 p. 1131 - 1136
反应条件
in pyridine; dichloromethane 15 h; Ambient temperature;
参考文献
Julia, Marc; Mestdagh, Helene
Tetrahedron, 1984 , vol. 40, # 2 p. 327 - 337
反应条件
in pyridine; dichloromethane
15 h; Ambient temperature;
参考文献
Julia, Marc; Mestdagh, Helene
Tetrahedron, 1984 , vol. 40, # 2 p. 327 - 337
反应条件
1: 91 percent / triethylamine / CH2Cl2 / 7 h / 0 - 20 °C
2: 86 percent / sodium azide / dimethylformamide / 24 h / 85 °C
3: 91 percent / hydrogen; HCl / 20 percent palladium hydroxide / methanol; H2O / 8 h / 20 °C / 760 Torr
View Scheme
参考文献
Kuppert, Dirk; Sander, Juergen; Roth, Christian; Woerle, Michael; Weyhermueller, Thomas; Reiss, Guido J.; Schilde, Uwe; Mueller, Iris; Hegetschweiler, Kaspar
European Journal of Inorganic Chemistry, 2001 , # 10 p. 2525 - 2542
反应条件
Boc-L-(π-Me)-His-(A)Gly-L-Cha-L-Phe-OMe in toluene
T=-20°C; 9 h; Inert atmosphere; optical yield given as percent ee;
参考文献
Hrdina, Radim; Mueller, Christian E.; Wende, Raffael C.; Wanka, Lukas; Schreiner, Peter R.
Chemical Communications, 2012 , vol. 48, # 19 p. 2498 - 2500
