(±)-反-1,2-环戊二醇合成路线 （共 48 条）
反应条件
dihydrogen peroxide; toluene-4-sulfonic acid in water T=50°C; 21 h; Sealed flask;
参考文献
Rosatella, Andreia A.; Afonso, Carlos A.M.
Advanced Synthesis and Catalysis, 2011 , vol. 353, # 16 p. 2920 - 2926
反应条件
water; tetra(n-butyl)ammonium hydrogensulfate T=20 - 45°C;
参考文献
Fan, Ren-Hua; Hou, Xue-Long
Organic and Biomolecular Chemistry, 2003 , vol. 1, # 9 p. 1565 - 1567
反应条件
chloro-trimethyl-silane; zinc; Cp2Ti(Ph)Cl in tetrahydrofuran T=20°C; 38 h;
参考文献
Yamamoto; Hattori; Miwa; Nakagai; Kubota; Okamoto; Itoh
Journal of Organic Chemistry, 2001 , vol. 66, # 11 p. 3865 - 3870
反应条件
tetra-N-butylammonium borohydride in various solvent(s) T=25°C; Reduction;
参考文献
Gatling, Sterling C.; Jackson, James E.
Journal of the American Chemical Society, 1999 , vol. 121, # 37 p. 8655 - 8656
反应条件
chloro-trimethyl-silane; zinc; Cp2Ti(Ph)Cl in tetrahydrofuran 38 h; Ambient temperature; Yield givenYields of byproduct given. Title compound not separated from byproducts;
参考文献
Yamamoto, Yoshihiko; Hattori, Reiko; Itoh, Kenji
Chemical Communications, 1999 , # 9 p. 825 - 826
反应条件
dihydrogen peroxide; WO3; silica gel in tert-butyl alcohol T=34.85°C; 24 h; Product distribution; Further Variations:CatalystsSolvents;
参考文献
Jin, Ronghua; Li, Hexing; Deng, Jing-Fa
Journal of Catalysis, 2001 , vol. 203, # 1 p. 75 - 81
反应条件
water; hydrogen; platinum(IV) oxide 1.) acetone, pH 8.0, 2.) ethanol, 12 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Ross, Angela M.; Pohl, Terese M.; Piazza, Kathryn; Thomas, Michael; Fox, Bonnie; Whalen, Dale L.
Journal of the American Chemical Society, 1982 , vol. 104, # 6 p. 1658 - 1665
参考文献
Godchot; Taboury
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1912 , vol. 154, p. 1625
Bulletin de la Societe Chimique de France, 1913 , vol. <4> 13, p. 536
反应条件
ethanol; platinum Hydrogenation;
参考文献
Criegee; Beucker
Justus Liebigs Annalen der Chemie, 1939 , vol. 541, p. 218,225
Full Text Show Details
Criegee
Justus Liebigs Annalen der Chemie, 1930 , vol. 481, p. 263,286
Chemische Berichte, 1931 , vol. 64, p. 260,264
反应条件
1: aluminium oxide /kieselguhr / 380 - 400 °C 2: SeO2; aqueous H2O2; tert-butyl alcohol View Scheme
参考文献
Stoll et al.
Helvetica Chimica Acta, 1953 , vol. 36, p. 268,273
