2-(烯丙氧基)乙基 4-甲基苯磺酸盐合成路线 （共 9 条）
反应条件
ethylene dibromide; magnesium bromide in diethyl ether Ambient temperature;
参考文献
Okabe, Masami; Tada, Masaru
Bulletin of the Chemical Society of Japan, 1982 , vol. 55, # 5 p. 1498 - 1503
反应条件
4-(N,N-dimethlyamino)pyridine; triethylamine in dichloromethane
T=0 - 20°C;
参考文献
Ayme, Jean-Francois; Lux, Jacques; Sauvage, Jean-Pierre; Sour, Angelique
Chemistry - A European Journal, 2012 , vol. 18, # 18 p. 5565 - 5573
反应条件
potassium carbonate in ethanol
18 h; Heating;
参考文献
Lankshear, Michael D.; Evans, Nicholas H.; Bayly, Simon R.; Beer, Paul D.
Chemistry - A European Journal, 2007 , vol. 13, # 14 p. 3861 - 3870
反应条件
sodium iodide in acetone
24 h; Heating;
参考文献
Okabe, Masami; Tada, Masaru
Bulletin of the Chemical Society of Japan, 1982 , vol. 55, # 5 p. 1498 - 1503
反应条件
1: 1.) NaH / 1.) DMF, room temperature, 1 h; 2.) DMF, 90 deg C, 2 h
2: 1) HCO2H; 2) aq. H2O2; 3) KOH / 1) H2O, 70-80 deg C, 10 min; 2) H2O, 25 deg C, 15 h; 3) H2O, 95 deg C, 10 min
View Scheme
参考文献
Roveri; Cavrini; Gatti; et al.
European Journal of Medicinal Chemistry, 1983 , vol. 18, # 6 p. 555 - 557
反应条件
1: 6-aminopurine With potassium carbonate in N,N-dimethyl-formamide
Heating;
2: 2-(allyloxy)ethyl tosylate in N,N-dimethyl-formamide
Heating;
参考文献
Petrov; Ozerov; Novikov; Pannecouque; Balzarini; De Clercq
Chemistry of Heterocyclic Compounds, 2003 , vol. 39, # 9 p. 1218 - 1226
反应条件
potassium carbonate
1.) DMF, 80 deg C, 1 h, 2.) DMF, 95-100 deg C, 12 h; Yield given. Multistep reaction;
参考文献
Ozerov; Novikov
Chemistry of Heterocyclic Compounds, 1996 , vol. 32, # 6 p. 712 - 715
反应条件
in dimethyl sulfoxide
T=90°C; 2 h;
参考文献
Roveri; Cavrini; Gatti
Farmaco, Edizione Scientifica, 1984 , vol. 39, # 4 p. 346 - 352
反应条件
in dimethyl sulfoxide
T=90°C; 2 h;
参考文献
Novikov, M. M.; Brel', A. K.; Ozerov, A. A.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1993 , vol. 29, # 3 p. 330 - 334
Khimiya Geterotsiklicheskikh Soedinenii, 1993 , # 3 p. 393 - 397
