2,3,4,5-四氢吡啶合成路线 （共 43 条）
反应条件
1: in tetrahydrofuran; toluene
T=-78 - 20°C; 48 h;
2: With hydrogen; palladium on activated charcoal in tetrahydrofuran; methanol; toluene
T=20°C; 12 h;
3: With hydrogenchloride; diethyl ether in tetrahydrofuran; methanol; toluene
Title compound not separated from byproducts;
参考文献
Wu, T. Robert; Chong, J. Michael
Journal of the American Chemical Society, 2006 , vol. 128, # 30 p. 9646 - 9647
反应条件
aqueous solution of pH 7-8
参考文献
Schoepf et al.
Chemische Berichte, 1956 , vol. 89, p. 1821,1823, 1831
Full Text Show Details
Schoepf; in K. Ziegler
Praeparative Organische Chemie Tl. II (= Naturf. Med. Dtdschld. 1939-1946, Bd. 37) <Weinheim 1953> S. 117, 121
反应条件
1: in tetrahydrofuran; toluene
T=-78 - 20°C; 48 h;
2: With hydrogen; palladium on activated charcoal in tetrahydrofuran; methanol; toluene
T=20°C; 12 h;
3: With hydrogenchloride; diethyl ether in tetrahydrofuran; methanol; toluene
Title compound not separated from byproducts;
参考文献
Wu, T. Robert; Chong, J. Michael
Journal of the American Chemical Society, 2006 , vol. 128, # 30 p. 9646 - 9647
