次氮基-氰基二硫基-甲烷合成路线 (共 120 条)
参考文献
Kaufmann; Ritter
Archiv der Pharmazie (Weinheim, Germany), 1929 , p. 227
反应条件
chloroform; chlorine
T=-60°C; anschliessend mit Aethylen;
参考文献
Angus; Bacon
Journal of the Chemical Society, 1958 , p. 774,777,778
反应条件
acetic acid
T=0°C; Irradiation.Sonnenlicht;
参考文献
Guy,R.G.; Thompson,J.J.
Tetrahedron, 1978 , vol. 34, p. 541 - 546
反应条件
lithium perchlorate
T=40°C; without LiClO4; Product distributionRate constantMechanism;
参考文献
Skorobogatova, E. V.; Grudzinskaya, E. Yu.; Afanas'ev, P. S; Kartashov, V. R.; Zefirov, N. S.; Caple, R.
Journal of Organic Chemistry USSR (English Translation), 1987 , vol. 23, p. 1814 - 1822
Zhurnal Organicheskoi Khimii, 1987 , vol. 23, # 10 p. 2052 - 2060
反应条件
in benzene
T=20 - 25°C; 24 h; Irradiation; Yield given. Yields of byproduct given;
参考文献
Guy, R. G.; Cousins, S.; Farmer, D. M.; Henderson, A. D.; Wilson, C. L.
Tetrahedron, 1980 , vol. 36, p. 1839 - 1842
反应条件
T=20 - 25°C; 1 h; Irradiation; Yields of byproduct given;
参考文献
Guy, R. G.; Cousins, S.; Farmer, D. M.; Henderson, A. D.; Wilson, C. L.
Tetrahedron, 1980 , vol. 36, p. 1839 - 1842
反应条件
in benzene
4 h; Ambient temperature; Title compound not separated from byproducts;
参考文献
Giffard, Michel; Cousseau, Jack; Gouin, Lucien
Journal of Organometallic Chemistry, 1985 , vol. 287, p. 287 - 304
参考文献
Liermain
Annales de Chimie (Cachan, France), 1954 , vol. <12> 9, p. 507,525
参考文献
Wizemann,T. et al.
Journal of Organometallic Chemistry, 1969 , vol. 20, p. 211 - 217
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Gmelin Handbook: Bi: Org.Verb., 1.3.3.2.4.3, page 72 - 78
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Gmelin Handbook: Bi: Org.Verb., 1.4.1.2.3, page 112 - 112
反应条件
in benzene
few hours at 5°C;
参考文献
Wizemann,T. et al.
Journal of Organometallic Chemistry, 1969 , vol. 20, p. 211 - 217
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Gmelin Handbook: B: B-Verb.3, 2.7.8, page 35 - 35