次氮基-氰基二硫基-甲烷合成路线 (共 120 条)
反应条件
Pr.5: Kaliumsulfid, Pr.6: Kaliumpolythionat, Pr.7: Kaliumthiosulfat, Pr.8: Kaliumcarbonat;
参考文献
Seel; Mueller
Chemische Berichte, 1955 , vol. 88, p. 1747,1750, 1754
反应条件
in tetrachloromethane Irradiation;
参考文献
Bacon,R.G.R.; Irwin,R.S.
Journal of the Chemical Society, 1961 , p. 2447 - 2454
反应条件
in dichloromethane T=-40°C; 1.) 1h, -40 deg C, 2.) 1h, room temperature;
参考文献
Burski, J.; Kieszkowski, J.; Michalski, J.; Pakulski, M.; Skowronska, A.
Tetrahedron, 1983 , vol. 39, # 24 p. 4175 - 4182
反应条件
iron(III) chloride in 1,2-dichloro-ethane 1.) -30 deg C, 15 min, 2.) 20 deg C, 1 h;
参考文献
Neidlein, Richard; Constantinescu, Take
Chemische Berichte, 1989 , vol. 122, p. 1003 - 1008
反应条件
in benzene T=20°C; 1 h; further temp., solvents, reaction times; also in the presence of Lewis acids, iron; also under irradiation; also with ammonium thiocyanate as reactant; Product distribution;
参考文献
Neidlein, Richard; Constantinescu, Take
Chemische Berichte, 1989 , vol. 122, p. 1003 - 1008
反应条件
in presence of iron; AlCl3, FeCl3 or SnCl4; Product distribution;
参考文献
Neidlein, Richard; Constantinescu, Take; Kohl, Matthias
Phosphorus, Sulfur and Silicon and the Related Elements, 1991 , vol. 59, # 1-4 p. 165 - 168
反应条件
in dichloromethane
T=-40°C; 1.) 1h, -40 deg C, 2.) 1h, room temperature;
参考文献
Burski, J.; Kieszkowski, J.; Michalski, J.; Pakulski, M.; Skowronska, A.
Tetrahedron, 1983 , vol. 39, # 24 p. 4175 - 4182
参考文献
Michalski; Wieczorkowski
Roczniki Chemii, 1957 , vol. 31, p. 585,595
Chem.Abstr., 1958 , p. 5283
参考文献
Guy,R.G.; Thompson,J.J.
Tetrahedron, 1978 , vol. 34, p. 541 - 546
反应条件
UV-Licht initierte Reaktionen.Irradiation;
参考文献
Bacon,R.G.R.; Irwin,R.S.
Journal of the Chemical Society, 1961 , p. 2447 - 2454
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Bacon et al.
Proceedings of the Chemical Society, London, 1959 , p. 304