次氮基-氰基二硫基-甲烷合成路线 （共 120 条）
反应条件
iodine in acetic acid 17 h;
参考文献
Cambie, Richard C.; Rutledge, Peter S.; Strange, Gary A.; Woodgate, Paul D.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , p. 553 - 565
反应条件
in dichloromethane T=-10°C; The effect of temperature was examined.; Product distribution;
参考文献
Lopusinski, A.; Luczak, L.; Michalski, J.
Tetrahedron, 1982 , vol. 38, # 5 p. 679 - 683
反应条件
in carbon disulfide reaction of AgCN with a solution of (SCN)2 in CS2;;
参考文献
Soederbaeck, E.
Liebigs Annalen der Chemie, 1919 , vol. 419, p. 217 - 322
Full Text Show Details
Gmelin Handbook: Ag: MVol.B3, 16.8.1.1, page 343 - 345
反应条件
in diethyl ether reaction of Ag with a solution of (SCN)2 in ether;; poor yield;
参考文献
Soederbaeck, E.
Liebigs Annalen der Chemie, 1919 , vol. 419, p. 217 - 322
Full Text Show Details
Gmelin Handbook: Ag: MVol.B3, 16.8.1.1, page 343 - 345
参考文献
Michalski; Wieczorkowski
Bulletin de l'Academie Polonaise des Sciences, Serie des Sciences Chimiques, 1957 , vol. <III> 5, p. 917,919
反应条件
fluorine in various solvent(s) T=-20°C; Yield given. Yields of byproduct given;
参考文献
Loesking, Oliver; Willner, Helge
Angewandte Chemie, 1989 , vol. 101, # 9 p. 1283 - 1284
反应条件
in further solvent(s) byproducts: (FCN)3; reactn. of a soln. of dirhodane in FCl2C-CClF2 with diluted F2 (F2:N2 0 1:10); cooled down to -183°C; solvent removed by condensation; mixt. condensed to aq. KOH-soln. at room temp. to remove SF4, SOF and (FCN)3; sepn. by fractionated condensation at -127°C, -140°C, -196°C;
参考文献
Loesking, Oliver; Willner, Helge
Angewandte Chemie, 1989 , vol. 101, # 9 p. 1283 - 1284
反应条件
aluminium rhodanide; diethyl ether; chloroform
参考文献
Soederbaeck
Acta Chemica Scandinavica (1947-1973), 1954 , vol. 8, p. 1851,1855
参考文献
Challenger; Wilkinson
Journal of the Chemical Society, 1922 , vol. 121, p. 93,101
反应条件
(i) PhLi, (ii) /BRN= 1740308/, benzene; Multistep reaction;
参考文献
Boltze,K.-H. et al.
Justus Liebigs Annalen der Chemie, 1967 , vol. 709, p. 63 - 69
