次氮基-氰基二硫基-甲烷合成路线 （共 120 条）
反应条件
Br2 in neat (no solvent, gas phase) gas-phase titration;
参考文献
Frost, D.C.; MacDonald, C.B.; McDowell, C.A.; Westwood, N.R.C.
Journal of the American Chemical Society, 1981 , vol. 103, # 15 p. 4423 - 4427
反应条件
in water reaction of CoO and HCNS in aqueous soln.;; no isolation of the product;;
参考文献
Porrett, R.
Schw. J., 1816 , vol. 17, p. 289 - 289
反应条件
in further solvent(s) byproducts: (FCN)3; reactn. of a soln. of dirhodane in FCl2C-CClF2 with diluted F2 (F2:N2 0 1:10); cooled down to -183°C; solvent removed by condensation; mixt. condensed to aq. KOH-soln. at room temp. to remove SF4, SOF and (FCN)3; sepn. by fractionated condensation at -127°C, -140°C, -196°C;
参考文献
Angewandte Chemie, , vol. 101, # 9 p. 1283 - 1284
参考文献
Farbenfabr. Bayer
Patent: DE959191 , 1956 ;
反应条件
in further solvent(s) byproducts: (FCN)3; reactn. of a soln. of dirhodane in FCl2C-CClF2 with diluted F2 (F2:N2 0 1:10); cooled down to -183°C; solvent removed by condensation; mixt. condensed to aq. KOH-soln. at room temp. to remove SF4, SOF and (FCN)3; sepn. by fractionated condensation at -127°C, -140°C, -196°C;
参考文献
Angewandte Chemie, , vol. 101, # 9 p. 1283 - 1284
反应条件
UV-Licht initierte Reaktionen.Irradiation;
参考文献
Bacon,R.G.R.; Irwin,R.S.
Journal of the Chemical Society, 1961 , p. 2447 - 2454
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Bacon et al.
Proceedings of the Chemical Society, London, 1959 , p. 304
参考文献
Gmelin Handbook: Bi: Org.Verb., 1.3.3.1.1, page 46 - 55
反应条件
in tetrachloromethane; water
参考文献
Gmelin Handbook: Na: SVol.3, 1.2.5, page 912 - 916
参考文献
Kaufmann; Gaertner
Chemische Berichte, 1924 , vol. 57, p. 933
参考文献
Guy,R.G.; Thompson,J.J.
Tetrahedron, 1978 , vol. 34, p. 541 - 546
