1,3,5-三(4-羧基苯基)苯合成路线 （共 15 条）
反应条件
n-butyllithium in tetrahydrofuran; hexane T=-60°C;
参考文献
Weber, Edwin; Hecker, Manfred; Koepp, Erich; Orlia, Wolfgang; Czugler, Matyas; Csoeregh, Ingeborg
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1988 , p. 1251 - 1258
反应条件
bis-triphenylphosphine-palladium(II) chloride in N,N-dimethyl-formamide T=90°C; electrochemical reaction;
参考文献
Jutand, Anny; Negri, Serge
European Journal of Organic Chemistry, 1998 , # 9 p. 1811 - 1821
反应条件
bis-triphenylphosphine-palladium(II) chloride in N,N-dimethyl-formamide T=90°C; electrochemical reaction;
参考文献
Jutand, Anny; Negri, Serge
European Journal of Organic Chemistry, 1998 , # 9 p. 1811 - 1821
反应条件
1: 97 percent / triflic acid / 1.5 h / 140 - 150 °C / in vacuo 2: 67 percent / dimethylformamide / Ambient temperature; electrolysis 3: 75 percent / PdCl2(PPh3)2 / dimethylformamide / 90 °C / electrochemical reaction View Scheme
参考文献
Jutand, Anny; Negri, Serge
European Journal of Organic Chemistry, 1998 , # 9 p. 1811 - 1821
反应条件
1: triethylamine / CH2Cl2 / -50 deg C (1 h) to r.t (8 h) 2: 97 percent / triflic acid / 1.5 h / 140 - 150 °C / in vacuo 3: 67 percent / dimethylformamide / Ambient temperature; electrolysis 4: 75 percent / PdCl2(PPh3)2 / dimethylformamide / 90 °C / electrochemical reaction View Scheme
参考文献
Jutand, Anny; Negri, Serge
European Journal of Organic Chemistry, 1998 , # 9 p. 1811 - 1821
反应条件
1: toluene-4-sulfonic acid; toluene View Scheme
参考文献
Svirbely; Weisberg
Journal of the American Chemical Society, 1959 , vol. 81, p. 257,259
反应条件
1: toluene View Scheme
参考文献
Svirbely; Weisberg
Journal of the American Chemical Society, 1959 , vol. 81, p. 257,259
反应条件
nitric acid T=160 - 180°C; im geschlossenen Rohr;
参考文献
Kothe,G.; Zimmermann,H.
Tetrahedron, 1973 , vol. 29, p. 2305 - 2313
参考文献
He, Yabing; Bian, Zheng; Kang, Chuanqing; Cheng, Yanqin; Gao, Lianxun
Tetrahedron, 2010 , vol. 66, # 19 p. 3553 - 3563
反应条件
1: 67 percent / dimethylformamide / Ambient temperature; electrolysis 2: 75 percent / PdCl2(PPh3)2 / dimethylformamide / 90 °C / electrochemical reaction View Scheme
参考文献
Jutand, Anny; Negri, Serge
European Journal of Organic Chemistry, 1998 , # 9 p. 1811 - 1821
