1: 92 percent / sulphuryl chloride / acetic acid / 3 h / Ambient temperature
2: 83 percent / Fremy's salt, K2HPO4 / H2O / 24 h / Ambient temperature
3: 39 percent / NaOH / H2O / 2 h / Heating
View Scheme
参考文献
Henderson, Graeme B.; Hill, Robert A.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , # 10 p. 2595 - 2599
sulfuryl dichloride in acetic acid
3 h; Ambient temperature;
参考文献
Henderson, Graeme B.; Hill, Robert A.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , # 10 p. 2595 - 2599
1.1: zinc(II) chloride / 20 °C
2.1: 1,1,1,3,3,3-hexamethyl-disilazane / 5 h / 140 °C
3.1: sodium hydride / tetrahydrofuran; mineral oil / 20 - 65 °C
3.2: 20 - 65 °C
4.1: hydrogenchloride / tetrahydrofuran; water / 16 h / 20 °C
View Scheme
参考文献
Koenigs; Rinker; Maus; Nieger; Rheinheimer; Waldvogel
Journal of Natural Products, 2010 , vol. 73, # 12 p. 2064 - 2066
Timonen, Juri M.; Nieminen, Riina M.; Sareila, Outi; Goulas, Antonis; Moilanen, Lauri J.; Haukka, Matti; Vainiotalo, Pirjo; Moilanen, Eeva; Aulaskari, Paula H.
European Journal of Medicinal Chemistry, 2011 , vol. 46, # 9 p. 3845 - 3850
