(4-morpholinyl)sulphenyl chloride in chloroform
3 h;
参考文献
Davis, Robert C.; Grinter, Trevor J.; Leaver, Derek; O'Neil, Robert M.; Thomson, Gordon A.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1990 , # 11 p. 2881 - 2887
pyridine in dichloromethane; chloroform
addn. of soln. of Pd-compd. in CHCl3 to soln. of org. compd. in CHCl3, stirring 3 h, evapn., extn. (Et2O, dimorpholinyl sulphide in this phase), stirring of ether-insoluble product with pyridine in CH2Cl2 (15 min); filtration to seperate the Methyldithioloisoquinolinium chloride, evapn. the CH2Cl2 soln., recrystn. (CH2Cl2-petroleum ether); elem. anal.;
参考文献
Davis, Robert. C.; Grinter, Trevor J.; Leaver, Derek; O'Neil, Robert M.; Thompson, Gordon A.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry, 1990 , p. 2881 - 2888
