in tetrahydrofuran stirring under Ar for 14h at room temp.; removing solvent and Fe(CO)5 in vac.; extn. residue (n-hexane); filtration; cooling red-brown soln. at -30°C overnight; elem. anal.;
参考文献
Diaz, Carlos
Polyhedron, 1990 , vol. 9, p. 1045 - 1050