反应条件
in tetrahydrofuran
byproducts: {(CH3)4N}Cl, CO; under N2; addn. of PhSbCl2 in THF to slurry of Ni-cluster in THF (5 min), color change cherry-red to deep red-brown, monitored by IR, 2 h, filtration, evapn. (brown powder), extn. (hexane, toluene, THF), addn. of PPNCl to THF extract; filtration, evapn. (brown powder), extn. (hexane, toluene, THF), evapn. of THF-extract, crystn. (concd. THF-soln. layering with cyclohexane);
参考文献
DesEnfants, Robert E.; Gavney, James A.; Hayashi, Randy K.; Rae, A. David; Dahl, Lawrence F.; Bjarnason, Asgeir
Journal of Organometallic Chemistry, 1990 , vol. 383, p. 543 - 572
