1,1-二乙基-3-甲基-3-亚硝基脲合成路线 (共 3 条)
反应条件
sulfuric acid; sodium nitrite in water
cooling;
参考文献
Snyder, John K.; Stock, Leon M.
Journal of Organic Chemistry, 1980 , vol. 45, # 5 p. 886 - 891
反应条件
sodium nitrite; sodium isothiocyanate
T=50°C; 18 h; pH 1.7, measurement of the formation of NOSCN; Rate constantMechanism;
参考文献
Singer, Sandra S.; Cole, Barbara B.
Journal of Organic Chemistry, 1981 , vol. 46, # 17 p. 3461 - 3466
反应条件
sodium isothiocyanate
T=50°C; 5 h; pH 3.3; Product distributionMechanism;
参考文献
Singer, Sandra S.; Cole, Barbara B.
Journal of Organic Chemistry, 1981 , vol. 46, # 17 p. 3461 - 3466