1,2,2,2-四氟乙基甲醚合成路线 (共 5 条)
反应条件
potassium hydroxide in carbon dioxide; water
参考文献
Anaquest, Inc.
Patent: US5205914 A1, 1993 ;
反应条件
N,N'-dimethyl-N,N'-propyleneurea; potassium hydroxide in various solvent(s)
1.) heating; 2.) 200 deg C, 1 h then 210 deg C, 1 h;
参考文献
Rozov, Leonid A.; Ramig, Keith
Tetrahedron Letters, 1994 , vol. 35, # 26 p. 4501 - 4504
反应条件
N,N'-dimethyl-N,N'-propyleneurea; potassium hydroxide in various solvent(s)
1.) heating; 2.) 200 deg C, 1 h then 210 deg C, 1 h;
参考文献
Rozov, Leonid A.; Ramig, Keith
Tetrahedron Letters, 1994 , vol. 35, # 26 p. 4501 - 4504
反应条件
in acetonitrile-D3
T=-78 - 20°C; Title compound not separated from byproducts;
参考文献
Suzuta, Tetsuya; Abe, Takashi; Sekiya, Akira
Journal of Fluorine Chemistry, 2003 , vol. 119, # 1 p. 3 - 8
参考文献
Zapevalov, A. Ya.; Filyakova, T. I.; Peschanskii, N. V.; Kodess, M. I.; Kolenko, I. P.
Journal of Organic Chemistry USSR (English Translation), 1989 , vol. 25, # 3.1 p. 441 - 445
Zhurnal Organicheskoi Khimii, 1989 , vol. 25, # 3 p. 492 - 497