N2-甲基-2,3-吡啶二胺合成路线 （共 19 条）
反应条件
1: 58 percent / acetic acid / 24 h / Heating 2: 100 percent / H2 / 5percent Pd/alumina / CH2Cl2 / 3 h 3: 91 percent / LiAlH4 / tetrahydrofuran / 0.5 h / Heating View Scheme
参考文献
Zecchini; Torrini; Paradisi
Journal of Heterocyclic Chemistry, 1985 , vol. 22, # 2 p. 313 - 318
反应条件
1: concentrated aqueous HCl 2: CuSO4 View Scheme
参考文献
v. Schickh et al.
Chemische Berichte, 1936 , vol. 69, p. 2593,2604
反应条件
in ethanol 1.5 h; Heating;
参考文献
Savelli, Francesco; Boido, Alessandro; Damonte, Gianluca
Journal of Heterocyclic Chemistry, 1996 , vol. 33, # 6 p. 1737 - 1742
反应条件
1: 67 percent / CH2Cl2 / 2 h / Heating 2: 29 percent / POCl3 / 1.5 h / Heating View Scheme
参考文献
TANIGUCHI, Takahiko; YOSHIKAWA, Masato; MIURA, Kasei; HASUI, Tomoaki; HONDA, Eiji; IMAMURA, Keisuke; KAMATA, Makoto; KAMISAKI, Haruhi; QUINN, John F.; RAKER, Joseph; CAMARA, Fatoumata; WANG, Yi
Patent: US2011/319394 A1, 2011 ;
反应条件
acetic acid in dichloromethane T=150°C; 0.5 h; Microwave irradiation;
参考文献
Macdonald, Jonathan; Oldfield, Victoria; Bavetsias, Vassilios; Blagg, Julian
Organic and Biomolecular Chemistry, 2013 , vol. 11, # 14 p. 2335 - 2347
反应条件
in dichloromethane
Carbonylation; 2 h; Heating;
参考文献
Oguchi; Wada; Honma; Tanaka; Kaneko; Sakakibara; Ohsumi; Serizawa; Fujiwara; Horikoshi; Fujita
Journal of Medicinal Chemistry, 2000 , vol. 43, # 16 p. 3052 - 3066
参考文献
A/S Ferrosan
Patent: US4873244 A1, 1989 ;
参考文献
Dudash Jr., Joseph; Zhang, Yongzheng; Moore, John B.; Look, Richard; Liang, Yin; Beavers, Mary Pat; Conway, Bruce R.; Rybczynski, Philip J.; Demarest, Keith T.
Bioorganic and Medicinal Chemistry Letters, 2005 , vol. 15, # 21 p. 4790 - 4793
反应条件
1: phosphorous oxychloride / dimethylformamide / 95 °C
View Scheme
参考文献
Dudash Jr., Joseph; Zhang, Yongzheng; Moore, John B.; Look, Richard; Liang, Yin; Beavers, Mary Pat; Conway, Bruce R.; Rybczynski, Philip J.; Demarest, Keith T.
Bioorganic and Medicinal Chemistry Letters, 2005 , vol. 15, # 21 p. 4790 - 4793
