2-乙基-1H-异吲哚-1,3(2H)-二酮合成路线 （共 56 条）
反应条件
1: thionyl chloride / 2 h / Reflux 2: potassium carbonate / tetrahydrofuran / Cooling with ice 3: potassium dihydrogenphosphate; Cp*Rh(MeCN)3[ClO4]2; silver carbonate / 1,1-dimethylpropan-1-ol / 24 h / 100 °C / 760.05 Torr View Scheme
参考文献
Du, Ya; Hyster, Todd K.; Rovis, Tomislav
Chemical Communications, 2011 , vol. 47, # 44 p. 12074 - 12076
反应条件
1: thionyl chloride / 2 h / Reflux 2: potassium carbonate / tetrahydrofuran / Cooling with ice 3: potassium dihydrogenphosphate; Cp*Rh(MeCN)3[ClO4]2; silver carbonate / 1,1-dimethylpropan-1-ol / 24 h / 100 °C / 760.05 Torr View Scheme
参考文献
Du, Ya; Hyster, Todd K.; Rovis, Tomislav
Chemical Communications, 2011 , vol. 47, # 44 p. 12074 - 12076
参考文献
Tingle; Brenton
Journal of the American Chemical Society, 1910 , vol. 32, p. 115
反应条件
in acetonitrile Cyclization; elimination; 20 h; Irradiation;
参考文献
Yoon, Ung Chan; Lee, Chan Woo; Oh, Sun Wha; Mariano, Patrick S.
Tetrahedron, 1999 , vol. 55, # 41 p. 11997 - 12008
反应条件
1: 65 percent / acetonitrile / 30 h / Irradiation 2: 32 percent / acetonitrile / 20 h / Irradiation View Scheme
参考文献
Yoon, Ung Chan; Lee, Chan Woo; Oh, Sun Wha; Mariano, Patrick S.
Tetrahedron, 1999 , vol. 55, # 41 p. 11997 - 12008
反应条件
hydrogenchloride; water
参考文献
Koermendy
Acta Chimica Academiae Scientiarum Hungaricae, 1958 , vol. 17, p. 255,261
参考文献
Spring; Woods
Journal of the Chemical Society, 1945 , p. 625,627
参考文献
Kantlehner, Willi; Maier, Thomas; Loeffler, Wolfgang; Kapassakalidis, Joanis J.
Liebigs Annalen der Chemie, 1982 , # 3 p. 507 - 529
参考文献
Losse et al.
Journal fuer Praktische Chemie (Leipzig), 1958 , vol. <4>7, p. 28,33
反应条件
2: ethanolic sodium ethylate 3: water; hydrochloric acid View Scheme
参考文献
Koermendy
Acta Chimica Academiae Scientiarum Hungaricae, 1958 , vol. 17, p. 255,261
