4'-甲基-3-苯基苯丙酮合成路线 (共 34 条)
反应条件
potassium hydroxide; cis-[RuCl2(dimethylsulfoxide-S)3(dimethylsulfoxide-O)] in 1,4-dioxane T=80°C; 24 h;
参考文献
Martinez, Ricardo; Ramon, Diego J.; Yus, Miguel
Tetrahedron, 2006 , vol. 62, # 38 p. 8988 - 9001
反应条件
hydrogen; W-2 Raney nickel in ethyl acetate 0.5 h; Ambient temperatureIrradiation;
参考文献
Wang, Hui; Lian, Hongzhen; Chen, Jijun; Pan, Yi; Shi, Yaozeng
Synthetic Communications, 1999 , vol. 29, # 1 p. 129 - 134
反应条件
benzaldehyde; potassium hydroxide T=110°C; 32 h; Schlenk techniqueInert atmosphereGreen chemistry;
参考文献
Xu, Qing; Chen, Jianhui; Liu, Quan
Advanced Synthesis and Catalysis, 2013 , vol. 355, # 4 p. 697 - 704
反应条件
palladium 10 on activated carbon; sodium carbonate in ethanol; water T=100°C; Heck Reaction; 6 h;
参考文献
Kim, Hyun-Soo; Lee, Sang-Jin; Yoon, Cheol Min
Bulletin of the Korean Chemical Society, 2013 , vol. 34, # 1 p. 325 - 327
反应条件
C44H35ClO4P2Ru; potassium hydroxide in para-xylene T=130°C; 24 h; Inert atmosphereSchlenk techniqueMolecular sieve; Reagent/catalyst;
参考文献
Musa, Sanaa; Ackermann, Lutz; Gelman, Dmitri
Advanced Synthesis and Catalysis, 2013 , vol. 355, # 14-15 p. 3077 - 3080
反应条件
2,9-dimethyl-1,10-phenanthroline; palladium diacetate; copper(l) chloride in dimethyl sulfoxide T=50°C; P=760.051 Torr; 12 h; Reagent/catalystSolvent; regioselective reaction;
参考文献
Vellakkaran, Mari; Andappan, Murugaiah M.S.; Kommu, Nagaiah
Green Chemistry, 2014 , vol. 16, # 5 p. 2788 - 2797
反应条件
carbon monoxide T=150°C; Friedel-Crafts acylation; P=15201 Torr; 30 h;
参考文献
Ogoshi; Nakashima; Shimonaka; Kurosawa
Journal of the American Chemical Society, 2001 , vol. 123, # 35 p. 8626 - 8627
反应条件
2,9-dimethyl-1,10-phenanthroline; palladium diacetate; copper(l) chloride in dimethyl sulfoxide T=50°C; P=760.051 Torr; 12 h;
参考文献
Vellakkaran, Mari; Andappan, Murugaiah M.S.; Kommu, Nagaiah
Green Chemistry, 2014 , vol. 16, # 5 p. 2788 - 2797
反应条件
2,9-dimethyl-1,10-phenanthroline; palladium diacetate; copper(l) chloride in dimethyl sulfoxide T=50°C; P=760.051 Torr; 12 h;
参考文献
Vellakkaran, Mari; Andappan, Murugaiah M.S.; Kommu, Nagaiah
Green Chemistry, 2014 , vol. 16, # 5 p. 2788 - 2797
反应条件
potassium hydroxide; tris(triphenylphosphine)ruthenium(II) chloride in 1,4-dioxane T=80°C; 40 h;
参考文献
Cho, Chan Sik; Shim, Sang Chul
Journal of Organometallic Chemistry, 2006 , vol. 691, # 20 p. 4329 - 4332