6-氧代-环己-1-烯基乙酸酯合成路线 (共 12 条)
反应条件
Pd-BaSO4; ethanol Hydrogenation.anschliessende Verseifung mit methanol.HCl;
参考文献
Rosenmund et al.
Chemische Berichte, 1959 , vol. 92, p. 494,499
反应条件
D-glucose in water T=33°C; 24 h; Microbiological reaction; optical yield given as percent ee;
参考文献
Monsalve, Leandro N.; Cerrutti, Patricia; Galvagno, Miguel A.; Baldessari, Alicia
Biocatalysis and Biotransformation, 2010 , vol. 28, # 2 p. 137 - 143
反应条件
D-glucose in water T=33°C; 24 h; Microbiological reaction; optical yield given as percent ee;
参考文献
Monsalve, Leandro N.; Cerrutti, Patricia; Galvagno, Miguel A.; Baldessari, Alicia
Biocatalysis and Biotransformation, 2010 , vol. 28, # 2 p. 137 - 143
参考文献
Svennebring, Andreas; Garg, Neeraj; Nilsson, Peter; Hallberg, Anders; Larhed, Mats
Journal of Organic Chemistry, 2005 , vol. 70, # 12 p. 4720 - 4725
反应条件
D-glucose in water T=33°C; 24 h; Microbiological reaction; optical yield given as percent ee;
参考文献
Monsalve, Leandro N.; Cerrutti, Patricia; Galvagno, Miguel A.; Baldessari, Alicia
Biocatalysis and Biotransformation, 2010 , vol. 28, # 2 p. 137 - 143
参考文献
Monsalve, Leandro N.; Cerrutti, Patricia; Galvagno, Miguel A.; Baldessari, Alicia
Biocatalysis and Biotransformation, 2010 , vol. 28, # 2 p. 137 - 143
反应条件
triethylamine in dichloromethane
T=0 - 20°C;
参考文献
Svennebring, Andreas; Garg, Neeraj; Nilsson, Peter; Hallberg, Anders; Larhed, Mats
Journal of Organic Chemistry, 2005 , vol. 70, # 12 p. 4720 - 4725
反应条件
acetic acid in acetic anhydride
参考文献
Bordwell,F.G.; Wellman,K.M.
Journal of Organic Chemistry, 1966 , vol. 31, p. 351 - 357
反应条件
(i) MeC(OMe)3, TsOH, (ii) /BRN= 1744463/, TsOH; Multistep reaction;
参考文献
Becsi,F.; Zbiral,E.
Monatshefte fuer Chemie, 1979 , vol. 110, p. 955 - 978
反应条件
sodium acetate; palladium diacetate; ethylene glycol; poly(ethylene glycol) in water; acetonitrile
T=150°C; 0.333333 h; microwave irradiation;
参考文献
Svennebring, Andreas; Garg, Neeraj; Nilsson, Peter; Hallberg, Anders; Larhed, Mats
Journal of Organic Chemistry, 2005 , vol. 70, # 12 p. 4720 - 4725