反应条件
1: 98 percent / silylation
2: 92 percent / diisobutylaluminium hydride (DIBAL-H) / reduction
3: 1.) tricarbonyl(η6-arene)chromium(0) complex derived from (1R,2S)-N,N-dibutylnorephedrine, 2.)disibutylaluminium hydride (DIBAL-H) / 1.) toluene, hexanes, 0 deg C, 12 h, 2.) toluene, 23 deg C, 2 h
View Scheme
参考文献
Jones; Heaton
Tetrahedron Asymmetry, 1993 , vol. 4, # 2 p. 261 - 272
