2-甲氧基-5-丙-2-烯基苯酚合成路线 (共 13 条)
参考文献
Greca, Marina Della; Monaco, Pietro; Pollio, Antonino; Previtera, Lucio
Phytochemistry (Elsevier), 1992 , vol. 31, # 12 p. 4119 - 4124
反应条件
1: ethanolic KOH / 80 - 90 °C 2: diethyl ether; xylene / Erhitzen des vom Aether befreiten Reaktionsgemisches auf 160grad bis 180grad View Scheme
参考文献
Hirao
Bulletin of the Chemical Society of Japan, 1936 , vol. 11, p. 179,181
反应条件
C22H46N4; palladium diacetate; Ca(OH)2 in N,N-dimethyl acetamide; water
T=20 - 50°C; 24 h; Inert atmosphere;
参考文献
Mino, Takashi; Kogure, Taketo; Abe, Taichi; Koizumi, Tomoko; Fujita, Tsutomu; Sakamoto, Masami
European Journal of Organic Chemistry, 2013 , # 8 p. 1501 - 1505
反应条件
caesium carbonate in 2,2,2-trifluoroethanol
18 h; Irradiation;
参考文献
Protti, Stefano; Fagnoni, Maurizio; Albini, Angelo
Organic and Biomolecular Chemistry, 2005 , vol. 3, # 15 p. 2868 - 2871
反应条件
1: 76 percent / NCS / acetonitrile / 336 h / 20 °C
2: 57 percent / Cs2CO3 / 2,2,2-trifluoro-ethanol / 18 h / Irradiation
View Scheme
参考文献
Protti, Stefano; Fagnoni, Maurizio; Albini, Angelo
Organic and Biomolecular Chemistry, 2005 , vol. 3, # 15 p. 2868 - 2871
反应条件
1: K2CO3 / acetone / 8 h / Heating
2: 1 h / Heating
View Scheme
参考文献
Greca, Marina Della; Monaco, Pietro; Pollio, Antonino; Previtera, Lucio
Phytochemistry (Elsevier), 1992 , vol. 31, # 12 p. 4119 - 4124
反应条件
diethyl ether; xylene
Erhitzen des vom Aether befreiten Reaktionsgemisches auf 160-180grad;
参考文献
Schoepf et al.
Justus Liebigs Annalen der Chemie, 1940 , vol. 544, p. 30,58
Full Text Show Details
Hirao
Bulletin of the Chemical Society of Japan, 1936 , vol. 11, p. 179,181
参考文献
Grignard
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1910 , vol. 151, p. 323
参考文献
Greca, Marina Della; Monaco, Pietro; Pollio, Antonino; Previtera, Lucio
Phytochemistry (Elsevier), 1992 , vol. 31, # 12 p. 4119 - 4124
反应条件
Erhitzen des vom Aether befreiten Reaktionsgemisches auf 160-180grad;
参考文献
Schoepf et al.
Justus Liebigs Annalen der Chemie, 1940 , vol. 544, p. 30,58
Full Text Show Details
Hirao
Bulletin of the Chemical Society of Japan, 1936 , vol. 11, p. 179,181