反应条件
1: 94 percent / 2,6-lutidine / CH2Cl2 / 2 h / 0 °C
2: 1.) 9-H-9-BBN, 2.) NaOMe, PdCl2(dppf) / 1.) THF, rt, 2 h, 2.) THF, reflux, 1 h
3: 90 percent / 9-iodo-BBN / hexane / Ambient temperature
View Scheme
参考文献
Fuerstner; Seidel
Journal of Organic Chemistry, 1997 , vol. 62, # 8 p. 2332 - 2336
