2,3,4,5-四氯苯甲酸合成路线 (共 15 条)
反应条件
sodium hydroxide T=200°C;
参考文献
Nordlander; Cass
Journal of the American Chemical Society, 1947 , vol. 69, p. 2679
反应条件
disodium salt of hydroquinone in N,N-dimethyl-formamide T=100°C; 10 h;
参考文献
Ramadas, Sukuru R.; Pillai, Chandrasekaran N.; Bakthavatchalam, Rajagopal
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1985 , vol. 24, p. 1059 - 1060
反应条件
sodium hydroxide in methanol; benzene
参考文献
Fray,G.I.; Saxton,R.G.
Tetrahedron, 1978 , vol. 34, p. 2663 - 2667
反应条件
1: isopentyl nitrite 2: aq. NaOH / methanol; benzene View Scheme
参考文献
Fray,G.I.; Saxton,R.G.
Tetrahedron, 1978 , vol. 34, p. 2663 - 2667
反应条件
acetic acid T=300°C;
参考文献
Tust
Chemische Berichte, 1887 , vol. 20, p. 2441
反应条件
sulfuric acid T=200°C;
参考文献
Harvey et al.
Journal of Applied Chemistry, 1954 , vol. 4, p. 325,328
反应条件
triethylamine T=230 - 240°C;
参考文献
Roedig,A. et al.
Chemische Berichte, 1970 , vol. 103, p. 1011 - 1021
反应条件
0.5 h; Ambient temperature;
参考文献
Christopher Buxton; Heaney, Harry
Tetrahedron, 1995 , vol. 51, # 13 p. 3929 - 3938
参考文献
Roedig,A. et al.
Chemische Berichte, 1974 , vol. 107, p. 920 - 928
参考文献
Nordlander; Cass
Journal of the American Chemical Society, 1947 , vol. 69, p. 2679