1-亚甲基-4-(1-甲基乙烯基)环己烷合成路线 （共 20 条）
反应条件
oxalic acid
T=140 - 150°C;
参考文献
Webb; Bain
Journal of the American Chemical Society, 1953 , vol. 75, p. 4279
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Isskenderow
Zhurnal Obshchei Khimii, 1937 , vol. 7, p. 1435
Chem. Zentralbl., 1938 , vol. 109, # I p. 337
反应条件
hydrogenchloride in methanol
0.25 h; Ambient temperature;
参考文献
Hosomi, Akira; Iguchi, Hirokazu; Sasaki, Jun-ichi; Sakurai, Hideki
Tetrahedron Letters, 1982 , vol. 23, # 5 p. 551 - 554
反应条件
o-nitrobenzenesulfonyl hydrazide; triphenylphosphine; diethylazodicarboxylate in tetrahydrofuran
-30 deg, 1 h; 23 deg C 30 min;
参考文献
Myers, Andrew G.; Zheng, Bin
Tetrahedron Letters, 1996 , vol. 37, # 28 p. 4841 - 4844
反应条件
acetophenone in benzene
Irradiation;
参考文献
Kropp,P.J.
Journal of the American Chemical Society, 1969 , vol. 91, p. 5783 - 5791
反应条件
boron trifluoride diethyl etherate; sodium cyanoborohydride in tetrahydrofuran
T=65°C; 8 h; Yield given. Yields of byproduct given;
参考文献
Srikrishna, Adusumilli; Viswajanani, Ranganathan; Sattigeri, Jitendra A.; Yelamaggad, Channabasaveshwar V.
Tetrahedron Letters, 1995 , vol. 36, # 13 p. 2347 - 2350
反应条件
benzoic acid methyl ester; trifluorormethanesulfonic acid in ethyl acetate
72 h; UV-irradiation;
参考文献
Moran, Joseph; Cebrowski, Pamela H.; Beauchemin, Andre M.
Journal of Organic Chemistry, 2008 , vol. 73, # 3 p. 1004 - 1007
反应条件
1: 64 percent / aluminium chloride / benzene / 3.5 h / 15 - 20 °C / without cat. at 80 deg C, 36 h
2: 72 percent / diethyl ether / 4 h / Heating
3: 78 percent / HCl / methanol / 0.25 h / Ambient temperature
View Scheme
参考文献
Hosomi, Akira; Iguchi, Hirokazu; Sasaki, Jun-ichi; Sakurai, Hideki
Tetrahedron Letters, 1982 , vol. 23, # 5 p. 551 - 554
反应条件
T=170°C; Diels-Alder Cycloaddition; 5 h; Inert atmosphere; Temperature;
参考文献
TOTAL RAFFINAGE MARKETING; MAZURELLE, Jean
Patent: WO2013/53740 A1, 2013 ;
Location in patent: Page/Page column 12 ;
反应条件
1: 72 percent / diethyl ether / 4 h / Heating
2: 78 percent / HCl / methanol / 0.25 h / Ambient temperature
View Scheme
参考文献
Hosomi, Akira; Iguchi, Hirokazu; Sasaki, Jun-ichi; Sakurai, Hideki
Tetrahedron Letters, 1982 , vol. 23, # 5 p. 551 - 554
反应条件
in ethanol
T=400°C; P=91206.1 Torr; 0.0194444 h; Product distribution; Further Variations:Temperatures;
参考文献
Chibiryaev; Yermakova; Kozhevnikov; Sal'nikova; Anikeev
Russian Chemical Bulletin, 2007 , vol. 56, # 6 p. 1234 - 1238
