2-氨基-1-(3,4-二羟基苯基)乙烷-1-酮合成路线 （共 16 条）
参考文献
Hoechster Farbw.
Patent: DE157300 ;
参考文献
Suzuki; Furukawa
Yakugaku Zasshi, 1952 , vol. 72, p. 308
Chem.Abstr., 1953 , p. 2133
反应条件
1: With hydrogenchloride in methanol; water
T=60 - 65°C; 3 - 4 h;
2: With hydrogenchloride in isopropyl alcohol
参考文献
NEON LABORATORIES LTD.; DALVI, Mahesh Bhagoji; KENNY, Rajesh Shashikant; KAWLE, Ganesh Ramachandra
Patent: WO2013/8247 A1, 2013 ;
Location in patent: Page/Page column 10 ;
反应条件
water; palladium
P=7355.08 Torr; Hydrogenation;
参考文献
Simonoff; Hartung
Journal of the American Pharmaceutical Association (1912-1977), 1946 , vol. 35, p. 306,308
反应条件
hydrogenchloride
T=110°C; 3 h;
参考文献
Andersen; Jacobsen; Roepstorff
Tetrahedron, 1980 , vol. 36, # 22 p. 3249 - 3252
参考文献
Stolz
Chemische Berichte, 1904 , vol. 37, p. 4151
Full Text Show Details
Hoechster Farbw.
Patent: DE155632 ;
反应条件
1: Locusta migratoria, Na2EDTA, O2 / Ambient temperature; 0.2M Na-acetate buffer, pH 5.5, overnight incubation
2: 6M HCl / 3 h / 110 °C
View Scheme
参考文献
Andersen; Jacobsen; Roepstorff
Tetrahedron, 1980 , vol. 36, # 22 p. 3249 - 3252
反应条件
hydrogenchloride; palladium
Hydrogenation;
参考文献
Bretschneider; Hoermann
Monatshefte fuer Chemie, 1953 , vol. 84, p. 1021,1030
参考文献
Bayer and Co.
Patent: DE189483 ;
反应条件
hydrogen iodide; acetic acid
参考文献
Tutin
Journal of the Chemical Society, 1910 , vol. 97, p. 2520
