4,6-二硝基-1,3-苯二胺合成路线 （共 36 条）
反应条件
1: With tin; Degussa F101 catalyst; hydrogen in ethanol T=80.5°C; P=15514.9 Torr; 2 h; AutoclaveInert atmosphere; 2: With hydrogenchloride in ethanol; water T=15°C;
参考文献
E I DU PONT DE NEMOURS AND COMPANY; GOLDFINGER, MARC B.; PELLENBARG, TIMOTHY
Patent: US2014/66629 A1, 2014 ;
Location in patent: Paragraph 0073-0075 ;
反应条件
hydrogenchloride; tin
参考文献
Ruggli; Fischer
Helvetica Chimica Acta, 1945 , vol. 28, p. 1270,1276
参考文献
Nietzki; Hagenbach
Chemische Berichte, 1887 , vol. 20, p. 334
参考文献
E. I. du Pont de Nemours and Company
Patent: US8143450 B1, 2012 ;
Location in patent: Page/Page column 18-19 ;
反应条件
ammonium hydroxide in water; ethylene glycol
T=130°C; P=735.572 Torr; 2 h; Inert atmosphere;
参考文献
E. I. DU PONT DE NEMOURS AND COMPANY; DHAWAN, Rajiv; RITTER, Joachim, C.
Patent: WO2012/88184 A1, 2012 ;
Location in patent: Page/Page column 24-25 ;
反应条件
1: HNO3+H2SO4
2: alcohol; ammonia / 150 °C
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参考文献
Nietzki; Schedler
Chemische Berichte, 1897 , vol. 30, p. 1667
反应条件
ethanol; ammonia
T=150°C;
参考文献
Ruggli; Fischer
Helvetica Chimica Acta, 1945 , vol. 28, p. 1270,1276
反应条件
ammonium acetate; ammonia
T=165 - 170°C;
参考文献
Dandegaonker,S.H.; Kanabur,V.V.
Monatshefte fuer Chemie, 1968 , vol. 99, # 4 p. 1467 - 1472
反应条件
ethanol; ammonia
T=160°C;
参考文献
Blanksma; Meerum Terwogt
Recueil des Travaux Chimiques des Pays-Bas, 1902 , vol. 21, p. 288
参考文献
Hodgson; Nixon
Journal of the Chemical Society, 1928 , p. 1881
