(噻吩-2-甲基)硫代]乙酸合成路线 （共 5 条）
反应条件
potassium hydroxide in methanol
T=20°C; Hydrolysis; 24 h;
参考文献
Mandai, Sasanka Sekhar; Chakraborty, Jhilmil; De Asish
Journal of the Chemical Society - Perkin Transactions 1, 1999 , # 18 p. 2639 - 2644
反应条件
1: 67 percent / AlCl3 / CH2Cl2 / 0.25 h / 20 °C
2: 76 percent / trifluoroacetic acid; pyridine-borane / CH2Cl2 / 1 h / 0 °C
3: 96 percent / KOH / methanol / 24 h / 20 °C
View Scheme
参考文献
Mandai, Sasanka Sekhar; Chakraborty, Jhilmil; De Asish
Journal of the Chemical Society - Perkin Transactions 1, 1999 , # 18 p. 2639 - 2644
反应条件
1: 76 percent / trifluoroacetic acid; pyridine-borane / CH2Cl2 / 1 h / 0 °C
2: 96 percent / KOH / methanol / 24 h / 20 °C
View Scheme
参考文献
Mandai, Sasanka Sekhar; Chakraborty, Jhilmil; De Asish
Journal of the Chemical Society - Perkin Transactions 1, 1999 , # 18 p. 2639 - 2644
参考文献
Ramadas, S. R.; Chandrakumar, Nizal S.
Phosphorus and Sulfur and the Related Elements, 1982 , vol. 13, p. 79 - 84
参考文献
Cagniant
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1949 , vol. 229, p. 1342
