反应条件
1: 2-iodopyridine N-oxide With isopropylmagnesium chloride lithium chloride complex in tetrahydrofuran
T=-40°C; Inert atmosphere;
2: N,N-dimethyl-formamide in tetrahydrofuran
T=-40°C; Inert atmosphere;
3: With water; ammonium chloride in tetrahydrofuran
参考文献
Duan, Xin-Fang; Zi-Qian, Ma.; Zhang, Fang; Zhang, Zhan-Bin
Journal of Organic Chemistry, 2009 , vol. 74, # 2 p. 939 - 942