1,2-二硫杂苊 S-氧化物合成路线 (共 4 条)
反应条件
3-chloro-benzenecarboperoxoic acid in dichloromethane
T=0 - 20°C; 2.5 h; Inert atmosphere;
参考文献
Grainger, Richard S.; Patel, Bhaven; Kariuki, Benson M.
Angewandte Chemie, International Edition, 2009 , vol. 48, p. 4832 - 4835
Angewandte Chemie, 2009 , vol. 121, p. 4926 - 4929
反应条件
titanium(III) chloride; dihydrogen peroxide in methanol; water
0.0833333 h; Ambient temperature;
参考文献
Oae, Shigeru; Nabeshima, Tatsuya; Takata, Toshikazu
Heterocycles, 1982 , vol. 18, p. 41 - 44
反应条件
sulphite in 1,4-dioxane; water
T=25°C; Rate constant;
参考文献
Boduszek, Bogdan; Kice, John L.
Journal of Organic Chemistry, 1982 , vol. 47, # 17 p. 3199 - 3207
反应条件
sodium acetate; 2-methylpropane-2-thiol; acetic acid in 1,4-dioxane; water
T=25°C; pH=7.44, other pH; Rate constantMechanism;
参考文献
Boduszek, Bogdan; Kice, John L.
Journal of Organic Chemistry, 1982 , vol. 47, # 17 p. 3199 - 3207