4'-羟基-3'-甲氧基苯乙酮合成路线 （共 147 条）
反应条件
water; acetic acid; N,N,N',N'-tetramethylguanidine in tetrahydrofuran; acetonitrile T=20°C;
参考文献
CARLSON, Erin E.; TRADER, Darci
Patent: US2014/107328 A1, 2014 ;
Location in patent: Paragraph 0284; 0289 ;
反应条件
methanesulfonic acid; phosphorous pentoxide T=90°C; Fries rearrangement; 5 h;
参考文献
Ghinet, Alina; Rigo, Benoit; Gautret, Philippe
Revue Roumaine de Chimie, 2012 , vol. 57, # 12 p. 1065 - 1072
反应条件
acetic acid in tetrahydrofuran; water; acetonitrile T=20°C; pH=7.5; 12 h;
参考文献
CARLSON, Erin E.; TRADER, Darci
Patent: US2014/107328 A1, 2014 ;
Location in patent: Paragraph 0284; 0286 ;
反应条件
dihydrogen peroxide in water; acetonitrile 0.5 h; Microwave irradiation; Reagent/catalyst;
参考文献
Badamali, Sushanta K.; Luque, Rafael; Clark, James H.; Breeden, Simon W.
Catalysis Communications, 2013 , vol. 31, p. 1 - 4
反应条件
ammonium formate; palladium 10 on activated carbon in water; ethyl acetate T=80°C; 2 h;
参考文献
SAMEC, Joseph; LUNDSTEDT, Anna; SAWADJOON, Supaporn; KAT2BIZ AB C/O INTERPARES KONSULT AB
Patent: WO2012/121659 A1, 2012 ;
Location in patent: Page/Page column 14 ;
反应条件
ammonium formate; palladium 10 on activated carbon in water; ethyl acetate T=80°C; 2 h;
参考文献
SAMEC, Joseph; LUNDSTEDT, Anna; SAWADJOON, Supaporn; KAT2BIZ AB C/O INTERPARES KONSULT AB
Patent: WO2012/121659 A1, 2012 ;
Location in patent: Page/Page column 14-15 ;
反应条件
hydrogen bromide 3 h; Heating;
参考文献
RICHTER GEDEON VEGYESZETI GYAR RT.
Patent: WO2006/61666 A2, 2006 ;
Location in patent: Page/Page column 22-23 ;
反应条件
dihydrogen peroxide in water; acetonitrile 0.5 h; Microwave irradiation;
参考文献
Badamali, Sushanta K.; Luque, Rafael; Clark, James H.; Breeden, Simon W.
Catalysis Communications, 2013 , vol. 31, p. 1 - 4
反应条件
dihydrogen peroxide in water; acetonitrile 0.5 h; Microwave irradiation;
参考文献
Badamali, Sushanta K.; Luque, Rafael; Clark, James H.; Breeden, Simon W.
Catalysis Communications, 2013 , vol. 31, p. 1 - 4
反应条件
2-F-octylethanethiol; potassium tert-butylate in N,N-dimethyl-formamide T=110°C; 2 h; Inert atmosphere;
参考文献
Kale, Bhima; Shinde, Ananta; Sonar, Swapnil; Shingate, Bapurao; Kumar, Sanjeev; Ghosh, Samir; Venugopal, Soodamani; Shingare, Murlidhar
Tetrahedron Letters, 2010 , vol. 51, # 23 p. 3075 - 3078
