3-羟基-4-甲基-2(3H)-噻唑硫酮合成路线 （共 7 条）
反应条件
potassium hydroxide in dichloromethane; water T=0°C;
参考文献
Barton, Derek H.R.; Crich, David; Kretzschmar, Gerhard
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1986 , p. 39 - 54
反应条件
1: 3-hydroxy-4-methyl-2(3H)-thiazolethione With potassium carbonate in acetone T=20°C; 2: acetyl chloride in acetone T=20°C;
参考文献
Hartung, Jens; Schur, Christine; Kempter, Irina; Altermann, Sabine; Stapf, Georg; Bergstraesser, Uwe; Gottwald, Thomas; Heubes, Markus
Tetrahedron, 2009 , vol. 65, # 36 p. 7527 - 7532
反应条件
1,4-diaza-bicyclo[2.2.2]octane; T3P® in dichloromethane; N,N-dimethyl-formamide T=41°C; Acetylation; 72 h;
参考文献
Hartung, Jens; Schwarz, Michaela
Synlett, 2000 , # 3 p. 371 - 373
反应条件
in pyridine; dichloromethane 1 h; Ambient temperature;
参考文献
Barton, Derek H. R.; Bridon, Dominique; Zard, Samir Z.
Tetrahedron, 1989 , vol. 45, # 9 p. 2615 - 2626
反应条件
in pyridine; dichloromethane 1 h; Ambient temperature;
参考文献
Barton, Derek H. R.; Bridon, Dominique; Zard, Samir Z.
Tetrahedron, 1989 , vol. 45, # 9 p. 2615 - 2626
反应条件
pyridine; 4-(N,N-dimethlyamino)pyridine in diethyl ether
0.333333 h; Ambient temperature;
参考文献
Barton, Derek H.R.; Crich, David; Kretzschmar, Gerhard
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1986 , p. 39 - 54
参考文献
Barton, Derek H. R.; Kretzschmar, Gerhard
Tetrahedron Letters, 1983 , vol. 24, # 52 p. 5889 - 5892
