2,2-二氯-4’-甲基苯乙酮合成路线 (共 25 条)
反应条件
water; sodium carbonate Heating;
参考文献
Mahato, S. B.; Podder, G.; Maitra, S. K.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1986 , vol. 25, p. 1263
参考文献
Rabcewicz-Zubkowski
Roczniki Chemii, 1930 , vol. 10, p. 541,545
Chem. Zentralbl., 1930 , vol. 101, # II p. 3273
反应条件
indium monobromide in tetrahydrofuran T=20°C; 24 h;
参考文献
Peppe, Clovis; Pavao Das Chagas, Rafael
Synlett, 2004 , # 7 p. 1187 - 1190
反应条件
indium monobromide in tetrahydrofuran T=20°C; 24 h; Title compound not separated from byproducts;
参考文献
Peppe, Clovis; Pavao Das Chagas, Rafael
Synlett, 2004 , # 7 p. 1187 - 1190
反应条件
chloro-trimethyl-silane; potassium nitrate in dichloromethane
T=60°C; 16 h;
参考文献
Prakash, G.K. Sxurya; Ismail, Rehana; Garcia, Jessica; Panja, Chiradeep; Rasul, Golam; Mathew, Thomas; Olah, George A.
Tetrahedron Letters, 2011 , vol. 52, # 11 p. 1217 - 1221
反应条件
1,3-Dichloro-5,5-dimethyl-2,4-imidazolidinedione in acetonitrile
T=20°C; 0.75 h; Inert atmosphere;
参考文献
Chen, Zizhan; Zhou, Bin; Cai, Huihua; Zhu, Wei; Zou, Xinzhuo
Green Chemistry, 2009 , vol. 11, # 2 p. 275 - 278
反应条件
PhMgI in tetrahydrofuran
T=20°C; 1 h; Inert atmosphere; Reagent/catalyst;
参考文献
Essa, Ali H.; Lerrick, Reinner I.; Tuna, Floriana; Harrington, Ross W.; Clegg, William; Hall, Michael J.
Chemical Communications, 2013 , vol. 49, # 27 p. 2756 - 2758
反应条件
Oxonereg;; potassium chloride in water; acetonitrile
T=20°C; 0.25 h;
参考文献
Madabhushi, Sridhar; Jillella, Raveendra; Mallu, Kishore Kumar Reddy; Godala, Kondal Reddy; Vangipuram, Venkata Sairam
Tetrahedron Letters, 2013 , vol. 54, # 30 p. 3993 - 3996
反应条件
aluminium trichloride
T=0 - 5°C;
参考文献
Mahato, S. B.; Podder, G.; Maitra, S. K.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1986 , vol. 25, p. 1263
反应条件
in tetrahydrofuran
T=20°C; 1 h; Inert atmosphere; Reagent/catalyst;
参考文献
Essa, Ali H.; Lerrick, Reinner I.; Tuna, Floriana; Harrington, Ross W.; Clegg, William; Hall, Michael J.
Chemical Communications, 2013 , vol. 49, # 27 p. 2756 - 2758